GCMS calibration data for sample AD29522, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\LBF.D Vial: 59 Acq On 2 Jan 2002 11:08 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Pentane, 3-methoxy- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 2.99 ug/1 2009590 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 3-methoxy- 102 C6H140 036839-67-5 25 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 1-But anamine, 3 -methyl- 87 C5H13N 000107-85-7 9 4 Silane, etramethyl- 88 C4H12Si 000075-76-3 9 'Abundance / Scan 280 (7.614 min): LBF.D (-) " 570 73

5000 43

7.20 7.4G 7.60 7.80 8.00 37, |, J 55,61 67 1...... 87 .........103............. 126 l/1/1/-/1/1//B/OT/CTTTTTCnnTInI." m/ Z 43.05 32.57% m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1793: Pentane, 3-methoxy- 73

5000 45 720 7.40 7.60 7.80 3.00 m/z 41.00 11.59% .......4,33,38— 55 m/z-> 10 20 30 40__ 50 60 70 80 90 100 110 120 130 Abundance #292: N-Ethylformamide 30 73 TTmrrrTm l 7.20 7.40 7.60 7.80 8.00 5000- m/z 45.05 11.26% 44 58

15 1 • I ' 1 • ' I 1 ' .1. .. i ■ ' ' ' i ' ' ' ' i ■ ' ' ' i ' ' ■ ' i ' ' ■ ' i 1 ' ' ' i ' ' -d-tnn/k.n । । । । । । । । । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #763: 1-Butanamine, 3-methyl- 30 7.20 7.40 7.60 7.80 8.00 m/z 71.00 7.05% 5000-

41 15 FTBBuu | 55 70 87 — TTTBB—Uf1—11,1—0——9—9B**mTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7 20 7.40 7.60 7.80 8.00

LBF.D GCMS1126.M . Wed Jan 16 15:07:50 2002 Page 1

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