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GCMS calibration data for sample AD29522, Jan 2002

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Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.

NYC-WTC_000036695–000036702

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC31O1\LBF.D Vial: 59 . Acq On 2 Jan 2002 11:08 pm Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 23:57 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 2099094 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 8131202 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.57 164 3965083 20.00 ug/1 0.00 29) Phenanthrene-diO 24.99 188 6090086 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 3783053 20.00 ug/1 0.00 44) Perylene-dl2 37.13 264 2166512 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 164815 2.46 ug/mL 0.00 Spiked Amount 5.000 Recovery = 49.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 287 N.D. 3) \ bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 12.59 117 178 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12)’Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1413 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.57 153 282 N.D. 24) 2,4-Dinitrotoluene 21.32 165 937 N.D. 25) Diethylphthalate 22.16 149 327 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBF.D GCMS1126.M Wed Jan 16 11:38:38 2002 Page 1

NYC-WTC_000036696

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