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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 8:42 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 974736 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3757823 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 1907103 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.99 188 2826578m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1747247 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1004792 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 152105 4.89 ug/mL 0.00 Spiked Amount 5.000 Recovery = 97.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.24 74 485 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.94 77 183 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1028 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.52 162 315 N.D. 20) Dimethylphthalate 20.29 163 1203 N.D. 21) 2,6-Dinitrotoluene 20.28 165 503 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.65 153 261 N.D. 24) 2,4-Dinitrotoluene 21.31 165 205 N.D. 25) Diethylphthalate 22.13 149 3131. N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBD.D GCMS1126.M Fri Jan 18 08:42:38 2002 Page 1

NYC-WTC_000018070

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NYC-WTC_000018070Source: NYC Law Department, mirrored locally

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