GCMS analysis results for sample AD29791, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD29791 conducted on January 9, 2002.

NYC-WTC_000037207–000037215

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN0302\29791.D Vial: 12 Acq On 3 Jan 2002 9:18 pm Operator: 209 GALOS Sample gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 22:07 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.52 152 796262 20.00 ug/1 -0.18 10) Naphthalene-d8 15.12 136 3058717 20.00 ug/1 -0.19 17) Acenaphthene-diO 20.39 164 1495974 20.00 ug/1 -0.19 29) Phenanthrene-diO 24.81 188 2200003 20.00 ug/1 -0.19 38) Chrysene-dl2 32.84 240 1249370 20.00 ug/1 -0.19 44) Perylene-dl2 36.90 264 732143 20.00 ug/1 -0.22

System Monitoring Compounds 37) 2,4-DDD 29.88 235 133497 5.52 ug/mL -0.19 Spiked Amount 5.000 Recovery = 110.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.19 128 988 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 2 0.74 165 304 N.D. 25) Diethylphthalate 21.92 149 1329 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29791.D GCMS1126.M Mon Jan 07 13:00:48 2002 Page 1

NYC-WTC_000037209

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GCMS analysis results for sample AD29792, Jan 2002 · Box DEP Box 22

NYC-WTC_000037126

Laboratory report documenting GCMS analysis of sample AD29792 conducted on January 9, 2002, by the DEP.

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