GCMS analysis results sample AD29460, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29460.D Vial: 19 Acq On : 12 Dec 2001 8:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.29 ug/1 930378. 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, /tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 278 (7,599 min): 29460.D (-) m/ z 72.9,5 100.00% 73

5000 43 1 7.20 7.40 7.60 7.80 8.00 1 ‘ 1 1 1 1 ‘ 1 1 ' 1 1 I ‘ 36 , |. I 5.5. n-1 67, 1 |.... 87 ..... 103........ ‘ 'i' m/ Z 43.00 26.72% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide । 30 73

5000 - ■ i ■ • • < i > 1 1 ‘ । • 58 7.20 7.40 7.60 7.80 8.00 44 m/ z 41.0.0 10.18% — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73

7.20 7.40 ′ 7.60 7.80 8.00 5000 m/z 44.95 9.72% 45 1.5 , , 53 59 ' ........................ • i » • ■ ■ i ■ ■ ■ ■ । > • । ■ i ■ ■ > > । > m/z-> 10 20 30 40 50 70 80 60 90 100 110 120 Abundance #49423:1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet Im TII0111T IT 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.16% 5000-

45

...... 3611 ' I ■ • ■ • I ■ ■ ' ‘ l ■ ■ • • I ■ 55 67. • I 1 rl 1 I ' 1 ' 'I ' 109115 miz- > 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29460.D GCMS1126.M Fri Dec 21 12:27:32 2001 Page 1

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