GCMS analysis comments, sample AD29089, December 2001

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Library Search Compound Report * Data File : C:\HPCHEM\1\DATA\DEC1001\29089.D Vial: 36 Acq On : 11 Dec 2001 10:48 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.59 ug/1 166230 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H1603 020324-32-7 90 2 2-Propanol,, l’-oxybis- 134 C6H14O3 000110-98-5 50 3 2-Butanol,/3, 3'-oxybis- 162 C8H18O3 054305-61-2 50 4 1-Propano], 2-(2-hydroxypropoxy) - 134 C6H1403 000106-62-7 42 Abundance Scan 696 (11.436 mln): 29089.D (-) 59

5000 45 73 103 I “ ■ l TT T 11.20 11.40 11.60 11.80

miz-? 20 ■ i ■1 ■ ■ i • 30 -391— 40 IH 50 60 m 70 — 85 . 11 11 1 TT 1 I T 80 [ 1 ‘ ‘ 1 ■ i 1 1 • ■ i • ' • ■ i ■ • ■ ■ i ■ 90 100 110 120 130 140 m/z 45.00 41.36% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 73 11.20 11.40 11.60 11.80 31 m/z 103.05 32.32% --------+ |.... , 1 ।.... ।.... । r । ■ I • ‘‘‘I••■ 130 ■ i ■ ■ • ■ i • miz-> 20 30 40 50 160 70 80 90 100 110 120 130 140 Abundance #6087; 2-Propanol, 1,1-oxybis- 59

31 1120 1140 11.60 1180 ’

AC 5000 45 m/z 73.00 27.64% 103 89 72 — -P TPTT T}BmTTpTu—Ti '1 । । • ■ • • । • i ■ ■ । ‘ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3’oxybis- 59 11.20 11.40 11.60 11.80 m/z 41.05 22.68%

m/z~> 5000

TIT 20 31

—30PP 40 r TIT । r 50 45

(80 103

ge TTT 1——] TT TO—BTIr TT21111TT r 70 80 90 100 110 120 134 130 140 44 NA 11.20 11.40 11.60 11.80

29089.D GCMS1126.M Wed Dec 12 15:53:20 2001 Page 2

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