GCMS blank results for sample AD29022, Dec 17 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\LB.D Vial: 3 Acq On : 10 Dec 2001 11:42 am Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.42 0.88 ug/1 209467 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3 ‘-oxybis- 162 C8H18O3 054305-61-2 50 3 1-Propanol, 2- (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 39 Abundance 7 Scan 695 (11.422 mln): LB.D (-) m/z 59.05 100.00% 59

5000 45 103 73 ’ * I • * 11.00 11.20 11.40 11,60 11.80 T-pr-r-r-r-p-r 1 31151 84 1 fr'ii ■ । ■ ----- Tm——TT—IITGTIIISOI1O9ICI—CI‘TT m/z 44.9.5 48.22%

UA miz-2 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance ' #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 i • • r ■ i • ■ 111 ■ • ■' । ■ ■ ■ ■ । ■ 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 37.54%

miz—> Abundance

5000 I IT I TI- 20 30

31 40 —PT TI ............................................................... 50 60 70 80 90 100 110 120 130 140 #12859:2-Butanol, 3,3°-oxybis- 59 U 1—— TT ‘ 1 1 1 1 1 * • * I i » 11.00 11.20 11.40 11.60 11.80 m/z 73.00 29.77%

N 45 103

........ ‘ | • •................. • 1 • • • | • I............... ! . j......................................... , । i j . . ............................. rp 1I 11111111111 , . , p m/z-> 20 30 40 50 60_ 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 242-hydroxypropoXy} 11 I J I I T IT —f T I"T I il j I J ' 11.00 11.20 11.40 11.60 11.80 m/z 41.0 5 22.49% 5000 A 31 ( 45 103

75 89 V ----- T+ I—r ‘191 —1101000001 TImuuuur 11f, p- PPMIA? 3 I J 11 113 T I T } m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

LB.D GCMS1126.M Thu Dec 13 10:55:15 2001 Page 3

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