GCMS sample analysis AD29296, Dec 2001

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Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036278–000036288

Folder label: “GCMS X 12/4/01 A 12/10/01”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\DEC10 01\29455.D Vial: 6 Acq On 12 Dec 2001 4:37 am Operator: 209 GALOS Sample gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration .Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.41 1.13 ug/1 346224 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3/-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1/(2-methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 2-Propanol, 1, 1' -oxybis- 134 C6H14O3 000110-98-5 50 'Abundance Scan 694 (11.413 min): 29455.D (-) m/z 59.05 100.00% 59

5000-

-PPP 39 ll - 45

. .... T • । ■ ■ ■ • । ■ — 73

89 103

11.00 m/z N l • ■ ■ • l • ' ■ • l 11.20 45.00 11.40 11.60 11.80 52.28% m/z—> 20 30 40 50 60 70 80 90 100 110 120’ 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z .103.05 34.92% i .......... , ................................... ............ ,................. ,130.......... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butancl, 3,3'oxybis- 59 । V 1T 11.00 11.20 11.40 11.60 11.80 5000- 31 45 m/ z 73.00 28.11% 103

m/z-> Abundance 20 I ।

#9233: 2-Propanol, 1-(2-methoxypropoxy)- 1 1 ' i ' ' ■ ' i ' ' ' ' i ' ■ ' ' i ' ' ' ' i ' ' ' ' i ' ' ' ' i ' ' ' ' i ' ' ' 1 i 1 ' 1 ' i ' ' ■ ' i 1 1 1 1 i ' ' ' ' i ' 30 40 50 60 70

59 80 90 100 110 120 130 134 140

11.00 m/z 11.20 41.05 U 11.40 UA I 1 1 T-r | 1 ■ ' ' I ' ' ' ' I ' ' 11.60 11.80 24.95% 5000

31 45 —....... ................................................................. 11' ■'' । I Hl 1 ।1 ■ ■ ’ । ■ m/z-> 20 30 40 50 60 70 80 90 100 116 120 130 140 11.00 11.20 11.40 11.60 11.80

29455.D GCMS1126.M Wed Dec 19 12:59:35 2001 Page 3

NYC-WTC_000036287

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GCMS sample analysis AD29455, Dec 2001 · Box DEP Box 22

NYC-WTC_000036289

Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 1.000