GCMS calibration table, December 2001

NYC 9/11 Public Portal Document

Library. Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2801\LB.D Vial: 2 Acq On : 28 Dec 2001 8:48 am Operator: GALOS Sample : gems unknown 11/28 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclohexane, methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.01 0.49 ng/uL 100760 1,4-Dichlorobenzene-d4 11.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 2 Cyclohexane, methyl - 98 C7H14 000108-87-2 78 3 1H-Pyrazole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 53 4 2-Pentene, 2,3-dimethyl - 98 C7H14 010574-37-5 40 Abundance Scan 18 (5.009 min): LB.D (-) m/z K 83.05 100.00% 63

41 98 5000 69 \_________________ T’T T‘Ir‘0 , TI‘1‘1111‘1111‘ TTT 4.90 5.00 5.10 5.20 5.30 5.40

m/z-> 20 25 30 35 36 .i 1 TP II+ n-rp- 40 ... Illi........ I - 45 50 55 60 65 70 75 80 85 90 95 100 105 T‘ ‘‘T m/z 55.10 97.86% 'Abundance #1326: Cyclohexane, methyl- 55 83

5000 98 r, , । .। T’ TT 42 4.90 5.00 5.10 5.20 5.30 5.40 27 69 m/ z 41.10 52.97% ■ । ■ ■ ■ • । • ' i " ■' i " " i1 ■ i ■ ■ •11 ■ THTmpin Tr - "T‘tt1.‘r1‘1‘111111ttfTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000 #63234: Cyclohexane, methyl- 55 83 NW A 4.90 5.00 5.10 5.20 5.30 5.40 m/z 98.15 I ' ' ' ' f

52.07% 42 98 69 27 i T‘‘‘‘T T-i | I ______________ . TTTTTT" 11' i " '' i " " i " " r " ■ i " ■11 ‘1 ■ ■ । ■ ■' TTT ■ i > ■ • ■i > m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1232: 1H-Pyrazole, 4,5-dihydro-4,5-dimethyl- I' ' ' * I ' ' I ' ' ' ' I ' ' ' ' I i ■ ■ ■ ' i 833 4.90 5.00 5.10 5.20 5.30 5.40 m/ z 42.10 34.27% 5000 42 98 56 27 ........ .......... TTTTTITTTTT > . । । । L। , * ' 11" 11 ' “Wmggu m-i j ) I I I | 69 +TTTT mpH 11." " I " A \ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40

LB.D NP112701.M Mon Dec 31 10:12:14 2001 Page 1

NYC-WTC_000035524