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← Document results/DEP Box 22/GCMS X 11/27/01 A 12/7/01
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GCMS analysis comments, sample AD28801, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28801 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate.

NYC-WTC_000035452–000035459

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

f Data File C:\HPCHEM\l\DATA\DEC0601\28801.D Vial: 28 Acq On 7 Dec 2001 2:01 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.669 717 722 750 rBV 2135635 5460505 72.47% 13.674% 2 15.277 1109 1115 1133 rBV 3335479 7176081 95.24% 17.970% 3 20.556 1683 1690 1698 rBV 3487094 7534500 100.00% 18.867% 4 24.972 2165 2171 2183 rBV2 3298541 7316228 97.10% 18.320% 5 25.118 2183 2187 2194 rVB2 29243 81264 1.08% 0.203%

6 30.048 2719 2724 2736 rBV 458791 916004 12.16% 2.294% 7 33.014 3038 3047 3071 rBV2 2545375 6102289 80.99% 15.281% 8 33.289 3072 3077 3089 rVB 59712 156604 2.08% 0.392% 9 37.108 3484 3493 3513 rBV 1820458 5191188 68.90% 12.999%

Sum of corrected areas: 39934663

28801.D GCMS1126.M Wed Dec 12 11:33:18 2001

NYC-WTC_000035457

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NYC-WTC_000035457Source: NYC Law Department, mirrored locally

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