GCMS comments for sample AD28477, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28477.D vial: 6 Acq On : 27 Nov 2001 10:10 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.50 ug/1 110533 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene-1/2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Biphenylene 152 C12H8 000259-79-0 9 4 Vanillin 152 C8H803 000121-33-5 9 Abundance Scan 710 (11.563 min): 28477.D (-) m/z 149.90 100.00% 150

5000 115 78 52 11.20 1140 11.60 11.80 ' ' 1111 3845.14 TTTTT66 — -- 87 1 1——— m/z 151.90 66.87% mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 1120 11.40 11.60 11.80 52 m/z 114.90 38.76%

miz-> 30 35 40 50 " I " " I " 60 70 87 11 T TIT 111. । । ■ 11J 11.■' 80 90 100 110 120 130 ...... . ■ 140 150 160 I——— Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 150 TT TT 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 21.63%

35 87 • ‘ | 1 ‘ | ‘ | I I "'i"" i" i ■ • ■ ■ i ■ ■ ■ ■ i > > • • । > J m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene TIt 0 1 1 152 1120 11.40 11.60 11.80 m/z 76.00 . 13.17% 5000

63 76

m/z—> — , ( 1 ......1 80 90 100 110 120 130 140 150 160 30 40 50 60 70 97 126 TIWTITT r‘‘t I I .. | I I I I | I I'l I | I | | | | | ! | I | 1 ■ i ■ ■ I T 11.20 11.40 11.60 11.80

28477.D GCMS1126.M Fri Nov 30 17:35:31 2001 Page 2

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