GCMS comments for sample AD28668, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report f Data File : C:\HPCHEM\1\DATA\NOV2901\28668.D Vial: 44 Acq On : 30 Nov 2001 5:13 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.51 ug/1 106938 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Acenaphthylene 152 C12H8 000208-96-8 9 4 Benzenebutanoic acid, 3-nitro-.gamm 223 C10H9NO5i ____ 006328-00-3 9 Abundance Scan 710 (11.560 min): 28668.D (-) m/z 149.90 100.00% 150

5000 115 52 78 Ii"

mz-> Abundance 30 ■ ■ i ■ 38 45 | -4-- 40 50 60 70 61 7. 80 90 #9593: 1,4-Dichlorobenzene-d4 - 100 110 120 130 140 150 160 I 1120 11.40 11.60 11.80 m/z 151.90 . 66.88%

KO

5000 115 78 11.20 11.40 11.60 11.80 ' 52 m/z 114.90 35.79%

m/z-> 30 35 40 50 T’T’T 60 70 ... .87,.... 80 90 100 110 120 130 — +........ — I 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- HO —iTTTTuueuuiuuuuun —ir 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.26%

35 87

miz-> I ' ' I 1 1 ' ■ i ' ' ' ' i 30 40 50 ■' 11'1 ■ i11 60 70 I i ' ' ' ' i ' ' • ■ i ■ ■ •' i ' ' 80 90 100 110 120 130 J' ..... 7487 iso*I iso Abundance #67015: Acenaphthylene TTOTTI—uuur 1TT । । r । > 152 1120 11.40 11.60 11.80 m/z 52.00 16.82% 5000

76 63 | PPPT P i i । i i । । । A i i । i i 87 98 ' 1 ................................. ( 126 . i ■ | I ■ 1 > | I IT 1 | 1 > I I ] II - m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28668.D GCMS1126.M Fri Nov 30 16:23:15 2001 Page 1

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