GCMS comments for sample AD28665, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2901\28665.D Vial: 42 Acq On : 30 NOV 2001 3:16 am Operator? 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params? LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 113115 1,4-Dichlorobenzene-d4 11.69 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene- 1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 Acenaphthylene 152 C12H8 000208-96-8 10 4 Benzoic acid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 Abundance L Scan 710 (11.565 min): 28665.D (-) m/z 149.90 100.00% 150

5000 115 78 52 TI TInmmndn , , TTTT > ■ i ■ 11.20 11.40 11.60 11.80

nfe-> 30 38 44 TI+Ht 63 i! 40 50 60 70 87 103 | ■ TT ■ ■11TTT 111 TH I i * ■ ■' i 80 90 100 110 120 130 140 150 160 1 1— m/z 151.90 , 66.45% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 , 1 ,,,,,, , TTT 1T , ,-p-T-T-T-r-r 78 11.20 11.40 11.60 11.80 52 m/z 114.90 37.05% 35 87 I ■ । ■ j > i ' '' ' i' ■ ' ■ i ' ■ +11PWTTIPPTTTT miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 TT , i > । —TTr TTr 115 11.20 11.40 11.60 11.80 5000 52 78 m/z78.05 . 18.73%

35 87 1 । । | i m । > , > . । I , •t ।' ।' 11'' > • ।' i 1-—— ‘O’’ mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67013: Acenaphthylene 152 11.20 11.40 11.60 11.80........ m/z 52.00 14.95% 5000

76 63 j TTTrTTTI_______ _______________ pill ( 1 | I ! 87 98 126 TITummmm 4-rrp- TIIT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28665.D GCMS1126.M Fri Nov 30 16:20:35 2001 Page 1

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