GCMS comments for sample AD28595, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0601\28594.D vial: 3 Acq On 6 Dec 2001 1:05 pm Operator: 209 GALOS Sample re extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.34 0.92 ug/1 337849 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1/(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3.3'-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Pentanol,/2-methyl - 102 C6H140 000590-36-3 42 4 1-Propanol; 2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 Abundance Scan 686 (11.343 min): 28594.D (-) m/z 59.05 100.00% 59

5000

— . 3411 45

—5150 . a60— 73

83 89 1 103

1TTTT ■ ■ ■ TT . । । । । ।।। . 130 M 11.00 11.20 11.40 11.60 m/z 44.95 43.72% 30 20 40 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

V 5000 TIIr T 45 103 11.00 11.20 11.40 11.60 73 31 m/ z 103.05 35.77% —PP T PIT .... —t —I- i ■ • ■ ■ । ■ ■ • 130 ■ । ‘ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 1 ' i 1 1 f । ... VA । । Ten PPTT 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 27.79% 45 103

— #4 ' i ' —+ h ।1111111111111111 —.... 134, m/z-> Abundance 20 30 40 50 60 70 80 90 100 #1763:2-Pentanol, 2-methyl- 110 120 130 140 V ■ ■ I ' T I ' ' ' ' I ' ' ' ' I • ' ' 1 I 59 11.00 11.20 11.40 11.60 m/z 41.05 23.52% 5000

N 45 27 87 69 V TITIITIH | > ■ ■ ''i • • • • । • — । .... । ri । > । > । TTTrmmr ■ ■ I ■ 1 ■ ■ P ' b ' I m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

28594.D GCMS1126.M Thu Dec 06 15:01:20 2001 Page 2

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