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GCMS analysis results for sample AD28049, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28049 conducted on January 2, 2002.

NYC-WTC_000034548–000034558

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28049.D Vial: 34 Acq On : 22 Dec 2001 12:17 am Operator: GALOS Sample : gems unknown 11/21 Inst. : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 5-Thiazolecarboxylic acid, 2,4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.62 0.85 ng/uL 191166 Perylene-dl2 37.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Thiazolecarboxylic acid, 2,4-dime 185 C8H11NO2S 007210-77-7 50 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 38 3 2-Undec e, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 38 4 2,4,6(Z ,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 23 Abundance Scan 3357 (35.623 min): 28049.D (-) m/z 185.10 100.00% 185 57

5000 70 43 112 83 98 35.20 35.40 35.60 35.80 36.00 143 166 281 111 11 m/z 57.10 76.31% miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #19120: 5-Thiazolecarboxylic acid, 2,4-dimethyl-, ethyl est 140 185 ........................................ ............... 71 5000 116 157 45 35.20 35.40 35.60 35.80 36.00 98 m/z 70.1,5 46.53%

miz-> ■ ■ i ■ ■ ' ' i ' • • ■ । ■ 1 > ■ । > । 40 60 80 I ' 1 1 1 I ■ ' L................. 100 120 140 160 180 200 220 240 260 280 Abundance #2667 Propereigic acid, hexyl-, diethyl ester 57 70 35.20 35.40 35.60 35.80 36.00 5000 112 m/z 71.15 43.63% 83

i :—42 . — ।., ;— 98 199 217 miz- 40__ 60 80 100 120 140 160 180 200 220 240 __________________________________ 260 280 Abundance #18485: 2-Undecene, 4,5-dimethyl- [R@,s@-(Z)]- 43 57 69 35.20 35.40 35.60 35.80 36.00

. L. m/z 43.10 36.26% 5000

83 98 112 140 - 182................................................ A AIT A-A—YAAAAM ■ ■ i ■ ' 11I1'' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 35.20 35.40 35.60 35.80 36.00

28049.D NP112701.M Thu Dec 27 08:39:37 2001 Page 2

NYC-WTC_000034557

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NYC-WTC_000034557Source: NYC Law Department, mirrored locally

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