GCMS unknowns analysis results for sample AD28326, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2601\28326.D Vial: 17 Acq On : 28 Nov 2001 9:54 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank I

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.52 ug/1 140029 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Biphenylene 152 C12H8 000259-79-0 9 4 2-Methyl- 6-nitroaniline _____ __ 152 C7H8N2O2 000570-24-1 9 Abundance Scan 710 (11.560 min): 28326.D (-) m/z 149.90 100.00% 150

5000 115 78 52 11.20 11.40 11.60 11.80

miz-> 3844 62 TTITTHHTTT 30 _1 40 50 60 70 80 + 90 100 110 120 130 140 150 — 87m 4 । ii. 111 ... ।

160 m/z 151.90 iiii 69.68% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 1120 1140 11.60 11.80 52 m/z 115.00 . 38.75% 87i 35 1 ■ i ■ ■ ■ ■ i'' ■ ‘ i —P IPPPPPTTPTTTT +TTPPTTT 11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9502: Benzere-1,2.3.4-d4-, 5.6-dichloro- 150 ■ i ■ ■ ■ ■ i ■ ■ TTT । । . 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 23.61%

35 87 ! 11111111.... । i TIT ' I III IjTI I ' i TTT ‘ i 1 1 ■' 11 . । । ■j m/z-> 30 40 50 ■' i' • ■ • i • ■ 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene 152 11.20 11,40 11.60 11.80 m/z 52.00 16.09% 5000 -

63 76 126 97

miz-> mm 30 40 50 60 70 TITTTTITTTTTTTTTTTTTTTTTTTTTT 1 80 90 100 110 120 130 140 150 160 • ।। ■ TTT । ■ ■ n >11111 11.20 11.40 11.60 11.80

28326.D GCMS1126.M Thu Jan 03 12:49:04 2002 Page 1

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