GCMS calibration table for TCLP analysis, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC1901\LBB.D Vial: 27 Acq On 19 Dec 2001 4:37 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 3

R. T. EstConc Area Relative to ISTD R.T.

6.29 0.42 ug/1 177368 1,4-Dichlorobenzene-d4 11.67

Hit:# of 5 entative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Pentanone, 2-methyl- 100 C6H120 000565-69-5 43 3 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 3(2H)-Furanone, dihydro-2-methyl- 100 C5H802 003188-00-9 35 Scan 136 (6.295 min): LBB.D (-) m/z43.05 . 100.00% 3 57

71 5000- 100

— ,.-AL । + 51 . 62 85 trHHTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT -ITTr m/z 6.00 6.20 57.00 6.40 6.60 79.68% 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 100 m/ z 71.00 53.04% 85 ETTu TTTTTT nz 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance tarone 57 43 ...... 6.00__ 6.20 6.40 ...6.60 5000- m/ z 100.05 32.04% 100 71 38 85 TTTTTT TUTTTTTTTTTTTUTTTCTCTTITTP 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abu • #732: Butane, 2,2-dimethyl- 43 57 6.00 6.20 6.40 6.60 71 m/ z 41.05 24.06% 29

.. AAA 5000

15 TTTTTT TTTTTTTTTTTT TTCEIEITTT TTTTTTETTTI’TT I j I H TT TTTTT m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60

LBB.D GCMS1126.M Wed Jan 02 12:10:25 2002 Page 1

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