GCMS analysis results for sample AD27549, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27549.D Vial: 8 Acq On : 13 Dec 2001 4:45 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C : \DATABASE\NBS75K . L

Peak Number 1 1-Butanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.18 0.50 ng/uL 162541 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 32 2 Cyanic aci , ethyl ester 71 C3H5NO 000627-48-5 5 3 Guanidine/ 59 CH5N3 000113-00-8 5 4 Isobutane 58 C4H10 000075-28-5 5 Abundance Scan 37 (5.185 min): 27549.D (-) m/ z 100.00% 41 56 59

5000- 71

45 “A —

m/z-> 10 15 20 25 30 35 + —... 4 40 45 50 55 4 TTICTTTETCI11 60 65 70 ' 1 i ■ • ' ■ i ' 75 80 5.00 m/z 5.20 56.10 5.40 5.60 77.74% Abundance #62584: 1-Butanol 41 56

5000- —I 14 4 ; 5.00 5.20 5.40 5.60 m/z 59.10 74.12% ----- 45 c 1— +53- m/z-> io 15 20 25 30 35__ 40 45 ______________ 50 55 60 65 70 75 80 Abundance #237: Cyanic acid, ethyl ester 29 56 5.00 X.-. —. 5.20 5.40 5.60 5000 71 m/z 4 .05 69.47% I 26 43 ________ ____ ll 40:____________ ■ • ■ l • • • ■ |•1 | •'• ■ । । n> . ।। । ।। । . 1 I 1 ' ' ’ I ' ( ( I ’ • i • ■ ■ ■ i ■ m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #100: Guanidine 43 59 5.00 5.20 5.40 5.60 m/z 42.05 60.97% 5000

17 27 31 - -----40 *PmmPunge | ■ ■ ■ ■ । ■ ■ ■ ■ । ■ TTTTIT AA — — ,A , m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 5.00 5.20 5.40 5.60

27549.D NP112701.M Fri Dec 14 12:56:42 2001 Page 1

NYC-WTC_000033498