GCMS header page dated December 13, 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\LB.D Vial: 2 Acq On : 13 Dec 2001 11:17 am Operator: GALOS Sample : gems unknown 11/15 Inst . : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.42 ng/uL 277153 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 90 3 2-Hexanone 100 C6H120 000591-78-6 78 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H1802 062338-17-4 74 'Abundance Scan 186 (6.549 min): LB.D (-) m/z 100.00% I 43 58 5000 - A TTmrrmi

m/Z~> 391 TPTTTTTTP l ThmpT T’’TTT — 1111' f 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71 85 100 6.20 m/ z 6.40

58 • 10 6.60 6.80 58.02% 7.00

Abundance #63384:2-Hexanone 43

5000- 58 IIPIT I T 6.20 6.40 6.60 6.80 7.00 29 m/z 57.05 16.30% 39 71 85 100 I ............... I' 1 " ।■ i1'' I' " • 111'' I' TTTTTT P •" I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000- 43 i I #1556:2-Hexanone

58 PTP 6.20 m/ z . AU. _ 6.40 41.10 6.60 6.80 14.99% 7.00

m/z-> Abundance

5000 - 27 39 i I 71 85 i 100 I " i" " r ■" r "' i" " r' " I ‘' i" " r " ‘ i" " i" " r •" i' ■111 ■ ■ ■ ■ I •" ■ r ■ " i " " I" " i ’"' i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #63386:2-Hexanone A, 6.20 6.40 m/z 100.05 MW 6.60 6.80 10.82% 7.00

58 29

m/z-> "r"■i• H TTTTTT 71 85 100 ' I'' " 11" ' i " " i " " I" " r 1" i' ■" I "1' i " ■ ■ I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 A,.. — A - 6.20 6.40 ■ 6.60 6.80 7.00

LB.D NP112701.M Fri Dec 14 12:59:11 2001 Page 1

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