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GCMS analysis results for sample AD27765, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27765 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033311–000033342

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial: 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 . MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.997 11 17 25 rW 643096 1715014 29.62% 4.864% 2 5.098 25 28 32 rW 152938 309447 5.34% 0.878% 3 5.162 32 35 52 rVB2 224342 570273 9.85% 1.617% 4 5.639 84 87 91 rW2 33387 59381 1.03% 0.168% 5 6.097 132 137 150 rBV 138423 345083 5.96% 0.979%

6 6.446 170 175 182 rBV 293390 599309 10.35% 1.700% 7 6.547 182 186 191 rBV 321302 548167 9.47% 1.555% 8 6.684 197 201 209 rBV 339744 692909 11.97% 1.965% 9 6.794 209 213 218 rW 353195 673371 11.63% 1.910% 10 6.904 222 225 231 rVB 33201 72917 1.26% 0.207%

11 7.014 233 237 241 rVB 35492 64830 1.12% 0.184% 12 7.757 313 318 322 rBV 245142 470318 8.12% 1.334% 13 7.831 322 326 341 rVB 862392 1768637 30.54% 5.016% 14 11.875 761 767 778 rVB 2184121 4495911 77.64% 12.751% 15 15.488 1155 1161 1179 rBV 2848979 5790722 100.00% 16.423%

16 20.760 1728 1736 1749 rBV 2653870 5634603 97.30% 15.981% 17 25.171 2205 2217 2225 rBV2 2450888 5288952 91.33% 15.000% 18 25.309 2228 2232 2238 rVB 27663 65688 1.13% 0.186% 19 33.177 3083 3090 3101 rVB2 1723348 3942642 68.09% 11.182% 20 37.257 3529 3535 3542 rVB2 804954 2150658 37.14% 6.100%

Sum of corrected areas: 35258832

27765.D NP112701.M Thu Dec 20 11:44:26 2001

NYC-WTC_000033330

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