GCMS analysis results for sample AD27764, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27764 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033285–000033310

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 2-Hexanol Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.97 ng/uL 246034 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 72 2 2-Pentanol, -methyl- 102 C6H140 000565-60-6 72 3 2—-Pentano Fenlanol, 3— methyl- 102 C6H140 000565-60-6 56 4 2 -Pentanol, 4-methyl-______ _ 102 C6H140 000108-11-2 56 •Abundance Scan 215 (6.811 min): 27764.D (-) m/z 45.10 100.. 00% 45

5000-

41 56 69 m -A — ! 84 87 6.40 6.60 6.80 7.00 7.20 72 +4 5341159 . ... I 1 H........... m/ z .05 19.84% m/z--> " ■' r' ■ i' ■ ■' i ■ "' i ■ ■ ■ ■ i" ■ ■ 11

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 +tt 41 W/ Abundance #63583: 2-Hexanol 45

5000- 44 6.40 6.60 6.80 7.00 7.20

69 m/z 44.05 18 ,69% i ■' ■ ■ । i ■ ■ • ■ i 27 31 3942, " " I" ‘I‘ Hn 55 58 TTTTNTNTI 1 84 87 rT •।■•••।• miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #63555: 2-Pentanol, 3-methyl- 45 TTdnnnum -- 6.40 6.60 6.80 7.00 7.20 5000 m/z 43.10 18 . 18%

27 30 56 15 31 3942 53 , 69 87 TTTWWWIWIPTTTWTTITWTTTTTIDTTT > a । ■ 11 । I 11 I 1111 l 11 11 11 I I | 11 . > । i ■ 11 ! . I . । । • < i ^ । > • miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 (Abundance #1777: 2-Pentanol, 3-methyl- --- i 45 6.40 6.60 6.80 7.00 7.20 m/z 69.10 14.65% 5000

41 56 A 27 mmmmm Ju tn-rp- 53, |, 69 TTe ‘ i11111'11 11'1 " I 11'11111' I " '' i1' 84 87 AAA m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27764.D NP112701.M Thu Dec 20 11:43:38 2001 Page 10

NYC-WTC_000033303

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GCMS analysis results for sample AD27639, Jan 2002 · Box DEP Box 21

NYC-WTC_000033221

Laboratory report documenting GCMS analysis of sample AD27639 for unknown compounds and surrogates on January 3, 2002.

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