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GCMS analysis results for sample AD27627, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27627 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033143–000033158

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

I. LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\DEC1901\27627.D Vial: 17 Acq On : 20 Dec 2001 12:30 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise :' Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.483 173 179 184 rBV 170701 330695 3.95% 0.752% 2 6.584 184 190 194 rBV 333380 660714 7.90% 1.503% 3 6.712 200 204 211 rVB 157643 277286 3.31% 0.631% 4 6.822 211 216 228 rVB 209269 405955 4.85% 0.923% 5 7.776 315 320 324 rBV 113365 204384 2.44% 0.465%

6 7.849 324 3 28 340 rVB 620986 1279018 15.29% 2.909% 7 8.565 402 406 412 rBV 46197 92452 1.11% 0.210% . 8 11.866 760 766 777 rVB 3083902 6347470 75.87% 14.436% 9 15.479 1152 1160 1177 rBV 3366016 8366177 100.00% 19.027% 10 20.752 1726 1735 1753 rBV 3343982 8198520 98.00% 18.645%

11 25.162 2208 2216 2226 rBV2 3223698 7683913 91.84% 17.475% 12 25.300 2226 2231 2237 rVB 34707 84939 1.02% 0.193% 13 33.168 3081 3089 3101 rBV2 2576915 6140913 73.40% 13.966% 14 35.680 3359 3363 3370 rBV2 41770 104879 1.25% 0.239% 15 37.258 3526 3535 3544 rBV2 1366224 3793325 45.34% 8.627%

Sum of corrected areas: 43970640

27627.D NP112701.M Fri Dec 21 09:18:03 2001

NYC-WTC_000033149

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NYC-WTC_000033149Source: NYC Law Department, mirrored locally

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