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GCMS analysis results for sample AD26678, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26678 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032007–000032027

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032025
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26678.D Vial: 4 Acq On 4 Dec 2001 1:33 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Cyclopentanecarboxylic acid, 2 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

29.57 0.59 ng/uL 135706 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 38 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 32 3 1-Hexene/ 2-methyl- 98 C7H14 006094-02-6 27 4 1-Undecene, 10-methyl- 168 C12H24 022370-55-4 16 [Abundance Scan 2697 (29.571 min): 26678.D (-) m/z 56.10 100.00%| iI 55 I

5000- 43 73 -

miz-> mp 20 40 , 6045 101117114. . 185 239 2 m/z 57.10 __ 80 100 120 140 160 180 200 220 240 260 29.20 29.40 29.60 29.80 30.00 47.29% Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 56

5000 LA -A- 1 I 29.20 29.40 29.60 29.80 30.00 m/z 43.10 44.76% 30 .. 69 82 100 129 1 I .1 42 ----- i •1 1 ■ । ' miz-> :20 40 60 __ 80 100 120 140 160 180 200 220 240 260 'Abundance #5218; Cyclopentanecarboxylic acid, 2-amino-, cis- 56 ‘d ■ I ' ' ' ' I ' 29.20 29.40 29.60 29.80 30.00 5000- m/z 41.10 39.30%

129 | 30 42 69 82 । 100 m/z-> Abundance 20 40 60 53 80 100 120 140 160 #1354: 1-Hexene, 2-methyl- 180 200 220 240 260 ____ AAA.... 29.20 29.40 29.60 29.80 30.00 m/z 55.10 32.11% 41 5000 - 27 70 I ' ’ ’ * I ' ' 1 , 1 83 ...... .... "d." m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 29.20 29.40 29.60 29.80 30.00

26678.D NP112701.M Fri Dec 07 13:08:55 2001 Page 11

NYC-WTC_000032025

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NYC-WTC_000032025Source: NYC Law Department, mirrored locally

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