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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26388.D vial: 14 Acq On 1 Dec 2001 12:02 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1,4-Dichlorobenzene-d4 Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.57 ng/uL 251345 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Di Chloroben:0ne-d4 150 C6C12D4 003855-82-1 95 2 Benzene-1,2,3, -d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42 3 Biphenylene j 152 C12H8 000259-79-0 9 4 2H-1-Benzopyra n-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 Abundance / Scan 753 (11.750 min): 26388.D (-) m/z 150.00 100.00% 150

5000 115 52 78 1140 11.60 11.80 1200.. —P +3 40 87 I ■ • i • m/z 152.00 I • TT. । । .1., । । . 67.29% mlz-> 30 70 80 4090 100 50 110 120 130 140 150 160 60 Abundance #9593:1,4-Dichlorobenzene-d4 150

115 ------- 5000 78 11.40 11.60 11.80 12.00 52 m/z 115.05 41.53%

miz-> 30 35 40 50 -r-r-p-n-r-p-r 87 111— 60 70 80 90 100 110 120 130 140 150 160 L.... Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 - 115 11.40 11.60 11.80 1200 5000- 52 78 m/z 78.05 , 26.44%

35 87 '....... |............. TT-p-m-p-r ............. I Illi I I I I I I I I I 1 I t : 1I miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene ____________ —■ ■ । । . k ______ । ■ rr । . . i । .... । i 152 11.40 11.60 11.80 12.00 m/z 52.00 22.55% 5000

63 76 126 — 97 .................................................. TIPTT - 1 ■ i * m/z—> 30 40 50 60 7‘ 80 90 100 110 120 130 140 150 160 । > । . . i । i i-t । r . j .... । i 11.40 11.60 11.80 12.00

26388.D NP112701.M Tue Dec 04 10:40:28 2001 Page 14

NYC-WTC_000031471

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NYC-WTC_000031471Source: NYC Law Department, mirrored locally

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