GCMS Analysis Report for Sample AD26388, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26388 .D vial: 14 Acq On 1 Dec 2001 12:02 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Pentanal, 2,2-dimethyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 10.53 2.15 ng/uL 947159 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 entative ID MW MolForm CAS# Qual 1 Pentanal ,2,2- dimethyl - 114 C7H140 014250-88-5 37 2 2-Hexanone, 3,3-dimethyl- 128 C8H160 026118-38-7 32 3 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 32 4 1-Pentanol, 2,2 - dimethyl - 116 C7H160 002370-12-9 17 Abundance Scan 620 (10.531 min): 26388.D (-) m/z 43.05 100.00% 43

5000

85 j ‘11/1/1/1/11 V 1112, 10.20 10.40 10.60 10.80 ----------30. .. ........................nil +mLOR m/z 45.10 30.85% miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3038: Pentanal, 2,2-dimethyl- 43

5000 —AA 10.20 10.40 10.60 10.80 85 m/z 41.10 24.62% 27 57 72

m/z—> 1111100215511117 wH 1mm] 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 —‘—11—00010000111 ^n-rq

Abundance #5126: 2-Hexanone, 3,3-dimethyl- 43 ' 1 i 1 r 111 10.20 10.40 10.60 10.80 5000 m/z 85.05 23.47% 85 15 27 mmlm Tmgap 1 m 57 69 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #637: Pyrrolidine, 3-methyl- / 1 ’ I ' ‘ * *7 ' ‘■ ■ i • ■ ■ ■ i 43 10.20 10.40 10.60 10.80 m/z 57.05 15.52% 5000 85

m/z—> 15 27 mmhmmkmmm1 Immphpmpn 56 68 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 .. j....j.... i*..। J A t i | : r : •[ J i I I j I I I i | I I i TI 10.20 10.40 10.60 10.80

26388.D NP112701.M Tue Dec 04 10:40:27 2001 Page 13

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