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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031152
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DECO401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 31.73 1.57 ug/1 433419 Chrysene-d12 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual ------------------=-------------------------------------------------- 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 37 2 Ethanedioic id, bis(trimethylsily 234 C8Hl8O4Si2 018294-04-7 35 3 Mercaptoace s.c acid, bis(trimethyls 236 C8H2002SSi2 006398-62-5 17 4 2-Hexened' is acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 17 Abundance Scan 2906 (31.725 min): 26205.D (-) I m/z 73.00 100. 00%

500& I 1 221 281 355 401 429 31.40 31.60 31.80 32.00 117 191 327 m/z 147.00 47. 1120140160180200220 4103: Trisiloxane, 1,1,1,5,

147

z 221.05 28. 117 207 10012014016018020022024 #71005: Ethanedioic acid, ester

I 31.40 31.60 31.80 32.00 m z 281.00 19.79%

117 _ ! 190

I Z 355. Ub 14.33''

221 45 1

A 60 80 100120140160180 1.40 31.60 31.80 3200

26205.D NP112601.M Tue Dec 04 15:59:03 2001 Page 15

NYC-WTC 000031152

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NYC-WTC_000031152Source: NYC Law Department, mirrored locally

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