GCMS analysis results for sample AE02604, Mar 15, 2002

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Data File C:\HPCHEM\l\DATA\MAR0702\2604.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

35.00 0.24 ug/1 46041 Chrysene-dl2 33.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1, ,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 3-1sopropoxy-1, ,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Mercaptoacetic bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 4 Ethanedioic aci bis(trimethylsily 234 C8H18O4Si2 018294-04-7 12 Abundance 3263 (34.999 min): 2604.D (-) m/z 7 3 """ 73

147 5000 221 281 355 I 429 34.60 34.80 35.00 35.20 35.40 44 - m/z 147.00 60.77% m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyi-3,3-bis[(trimet 73 147

5000- ■ ' i ' '

281 34.60 34.80 35.00 35.20 35.40 45 I 369 m/z 221.05 31.50% , J ) 117 . ..207 , 249 i.... t........... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73

K 34.60 34.80 35.00 35.20 35.40 5000- m/z 281.05 21.40% 147

221 281 327 415 519 561 ' ' I ' ' ' ' I ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 #30949: Mercaptoacetic acid, bis(trimethylsilyl)- MWAAAGWAInMt 34.60 34.80 35.00 35.20 35.40 147 m/z 355.05 21.31% 5000- 221 45 193 I J, .1 104 ' 1 I ■ ' ■ ' i ■ ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 34.60 34.80 35.00 35.20 35.40

2604.D GCMS0208.M Wed Mar 13 14:51:28 2002 Page 13

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