GCMS analysis results for sample AD26006, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Cycloheptene, methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

39.57 0.61 ng/uL 119874 Perylene-dl2 37.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cycloheptene, methyl- 110 C8H14 055308-20-8 22 2 Cycloheptene, methyl- 110 C8H14 055308-20-8 22 3 Cyclohexene, 1, 2-dimethyl- 110 C8H14 001674-10-8 14 4 Bicyclo[3.1 .0]hexan-3-ol, 4-methyle 152 C10H16O ________000471-16-9 10 'Abundance Scan 3787 (39.573 min): 26006A.D (-) m/z 55.10 100.00% 55 67 i 43 i 81 95 108 123 161 WWM\a/w wwhrvy 5000 176 231 215 191

m/z-> 20 1 1 1 1 ' '1 1 1 1 1 40 60 r-r-p 80 LW T‘ 100 149 I 120 140 ■160 180 200 I I 220 253 | 240 260 282 280 39.20 39.40 39.60 39.80 40.00 m/ z 67.10 88.58% 'Abundance #2367: Cycloheptene, methyl- 67 "WMMMVWw 81 95 5000 110 54 39.20 39.40 39.60 39.80 40.00 27 m/ z 43.10 76.59%

m/z-> 20 1 40 1 60 80 100 120 140 160 180 200 220 240 260 280 /W~w - Abundance #63885: Cycloheptene, methyl- 67

95 39.20 39.40 39.60 39.80 40.00 5000- 81 110 m/z 57.10 69.29%- 53 ! 27 I I WWN WwyA m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #63881: Cyclohexene, 1.2-dimethyl- 1 67 81 95 39.20 39.40 39.60 39.80 40.00 m/Z 161.10 66.69% 5000 - 110 53 li I | | l • • ■ • । ■ ■ • • । • ' • i • ' ‘ miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 39.20 39.40 39.60 39.80 40.00

26006A.D NP112701.M Thu Dec 20 10:40:01 2001 Page 9

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