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← Document results/DEP Box 18/GCMS X 5/17/02 A 5/16/02
Document / 9 pages

GCMS scan data for sample AE10812, May 2002

Machine-extracted title · confidence 100%

Fragmented GCMS scan data page showing tentative identification of compounds and surrogate recovery for sample AE10812.

NYC-WTC_000025533–000025541

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025533
OCR text

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY1302\10812.D Vial: 9 Acq On : 13 May 2002 11:42 pm Operator: Sample : GC/MS SCAN 5/7 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 28 14:25 2002

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title Last Update Response via DataAcq Meth : : : : 209 625/TCLP calibration table Fri May 17 11:28:42 2002 Initial Calibration GCMS0510 .... Jy A 2 VA — V y S CN V ,

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.16 152 550257 40.00 ug/1 -0.03 10) Naphthalene-d8 15.79 136 1981646 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.10 164 1089617 40.00 ug/1 -0.04 30) Phenanthrene-diO 25.54 188 1554683 40.00 ug/1 -0.03 38) Chrysene-dl2 33.62 240 1027077 40.00 ug/1 -0.02 44) Perylene-dl2 37.84 264 681680 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.24 209 26337 4. g/L -0.0 Spiked Amount 10.000 Recovery 48.60%

Target Compounds alue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.85 128 396 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.58 149 899 N.D. 26) 4-Chlorophenylphenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.54 178 378 N.D.

(#) = qualifier out of range (m) = manual integration 10812.D GCMS0510.M Tue May 28 14:26:14 2002 Page 1

NYC-WTC_000025533

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NYC-WTC_000025533Source: NYC Law Department, mirrored locally

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