NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAY1302\10812.D Vial: 9
Acq On : 13 May 2002 11:42 pm Operator:
Sample : GC/MS SCAN 5/7 Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 28 14:25 2002
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title
Last Update
Response via
DataAcq Meth
:
:
:
:
209 625/TCLP calibration table
Fri May 17 11:28:42 2002
Initial Calibration
GCMS0510
.... Jy
A 2
VA
—
V
y
S
CN
V
,
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.16 152 550257 40.00 ug/1 -0.03
10) Naphthalene-d8 15.79 136 1981646 40.00 ug/1 -0.04
17) Acenaphthene-diO 21.10 164 1089617 40.00 ug/1 -0.04
30) Phenanthrene-diO 25.54 188 1554683 40.00 ug/1 -0.03
38) Chrysene-dl2 33.62 240 1027077 40.00 ug/1 -0.02
44) Perylene-dl2 37.84 264 681680 40.00 ug/1 -0.02
System Monitoring Compounds
28) TCMX 23.24 209 26337 4. g/L -0.0
Spiked Amount 10.000 Recovery 48.60%
Target Compounds alue
2) N-nitrosodimethylamine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.85 128 396 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.58 149 899 N.D.
26) 4-Chlorophenylphenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzene 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 168 0 N.D.
32) 4-Bromophenylphenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
34) Phenanthrene 25.54 178 378 N.D.
(#) = qualifier out of range (m) = manual integration
10812.D GCMS0510.M Tue May 28 14:26:14 2002 Page 1
NYC-WTC_000025533
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