Gas chromatography-mass spectrometry report for sample AE10774 showing detection of unknown compounds and surrogate recovery.
NYC-WTC_000045869–000045877Folder label: “GCMS X 5/6/02 A 5/11/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\MAY1002\10774.D Vial: 18 Acq On : 11 May 2002 5:38 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 14:29 2002 Quant Results File: GCMS0510.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 12:35:42 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.17 152 544888 40.00 ug/1 -0.03 10) Naphthalene-d8 15.80 136 1984589 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.11 164 1096303 40.00 ug/1 -0.03 30) Phenanthrene-dlO 25.55 188 1527739 40.00 ug/1 -0.02 38) Chrysene-dl 2 33.62 240 1040646 40.00 ug/1 -0.02 44) Perylene-dl2 37.85 264 727628 40.00 ug/1 -0.01
System Monitoring Compounds 2 8) TCMX 23.25 209 42175 7.73 ug/L . 03 Spiked Amount 10,000 Recovery = 77.30%
Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.39 77 801 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.85 128 451 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.59 149 2508 N.D. 26) 4-Chlorophenylphenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.61 178 333 N.D.
(#) = qualifier out of range (m) = manual integration 10774.D GCMS0510.M Mon May 13 14:31:36 2002 Page 1
NYC-WTC_000045871
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