GCMS reference results for sample AE10772, May 2002

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Gas chromatography-mass spectrometry reference report for sample AE10772 listing measured values and detection limits.

NYC-WTC_000045849–000045858

Folder label: “GCMS X 5/6/02 A 5/11/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\10772.D Vial: 16 Acq On : 11 May 2002 3:41 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 14:03 2002 Quant Results File: GCMS0510.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 12:35:42 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.16 152 585653 40.00 ug/1 -0.03 10) Naphthalene-d8 15.80 136 2132628 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.11 164 1176251 40.00 ug/1 -0.03 30) Phenanthrene-diO 25.55 188 1626130 40.00 ug/1 -0.02 38) Chrysene-dl2 33.62 240 1099701 40.00 ug/1 -0.01 44) Perylene-dl2 37.85 264 760011 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.24 209 45270 7.74 ug/L -0.03 Spiked Amount 10.000 Recovery = 77.40%

Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.21 146 107 N.D. 5) 1,4-Dichlorobenzene 12.21 146 107 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.38 77 715 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.86 128 654 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.46 163 219 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.59 149 2571 N.D. 26) 4-Chlorophenylphenylether 0.00 204 0 N.D. 27) Fluorene 22.72 166 117 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.61 178 509 N.D.

(#) = qualifier out of range (m) = manual integration 10772.D GCMS0510.M Mon May 13 14:05:50 2002 Page 1

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GCMS analysis results for sample AE10773, May 2002 · Box DEP Box 25

NYC-WTC_000045859

Gas chromatography-mass spectrometry report for sample AE10773 showing detection of unknown compounds and surrogate recovery.

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