GC/MS analysis results, sample AE09766, May 15 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY1002\9766.D Vial: 11 Acq On : 10 May 2002 10:49 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 13 11:48 2002 <Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 13 08:58:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.17 152 618422 40.00 ug/1 -0.03 10) Naphthalene-d8 15.80 136 2213595 40.00 ug/1 -0.04 17) Acenaphthene-diO 21.10 164 1200646m 40.00 ug/1 -0.04 30) Phenanthrene-diO 25.55 188 1606824 40.00 ug/1 -0.03 38) Chrysene-dl2 33.61 240 954084 40.00 ug/1 -0.03 44) Perylene-dl2 37.83 264 606817 40.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 23.25 209 186326 31.20 ug/L -0.03 Spiked Amount 40.000 Recovery 78.00% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.32 74 1881 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.39 77 1007 N.D. 12) Isophorone 14.51 82 180 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.86 128 1093 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.37 162 173 N.D. 20) Dimethylphthalate 20.45 163 326 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.63 152 295 N.D. 23) Acenaphthene 21.19 153 230 N.D. 24) 2,4-Dinitrotoluene 21.37 165 366 N.D. 25) Diethylphthalate 22.59 149 1544 N.D. 26) 4-Chlorophenylphenylether 23.25 204 810 N.D. 27) Fluorene 22.72 166 294 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.25 168 508 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.61 178 440 N.D. (#) = qualifier out of range (m) = manual integration 9766.D GCMS0510.M Mon May 13 11:48:37 2002 Page 1

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