GC-MS chromatogram data, sample 11410, May 2002

NYC 9/11 Public Portal Document yuantitatlon Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\051702\0515REF2.D Vial: 18 Acq On : 18 May 2002 3:27 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 21 11:59:57 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 10007971 16.47 ug/L 98 38) Pyrene 27.17 202 10522220 17.46 ug/L 97 39) Butylbenzylphthalate 29.52 149 3368247 12.54 ug/L 93 40) Benzo(a)anthracene 30.78 228 7283393 15.18 ug/L 97 41) Bis(2-ethylhexyl)phthalate 31.38 149 4025994 11.09 ug/L 96 42) Chrysene 30.88 228 8369109m 16.84 ug/L 44) Di-n-octylphthalate 33.23 149 4366201 10.17 ug/L 99 45) Benzo(b)fluoranthene 33.75 252 6174040 17.53 ug/L 97 46) Benzo(k)fluoranthene 33.82 252 7524737 17.00 ug/L 99 47) Benzo(a)pyrene 34.54 252 4131231m 11.75 ug/L 48) Indeno(1,2,3-cd)pyrene 37.38 276 2953719 11.99 ug/L 99 49) Dibenz(a,h)anthracene 37.50 278 3902104 14.89 ug/L 99 50) Benzo(g,h,i)perylene 38.13 276 4179941 15.19 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0515REF2.D 050102.M Tue May 21 15:59:29 2002 Page 2

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