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← Document results/DEP Box 15/GCMS X 5/21/02 A 5/21/02
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GCMS calibration results, sample AE09517, May 22, 2002

Machine-extracted title · confidence 95%

Laboratory report showing calibration analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.

NYC-WTC_000013077–000013080

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document yuantitatlon Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\0 52102\CAL8 0.D Vial: 6 Acq On 21 May 2002 5:26 pm Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 22 14:45:47 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 22 14:45:43 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.52 202 35877771 74.10 ug/L 100 3 8) Pyrene 27.15 202 34971252 74.61 ug/L 100 39) Butylbenzylphthalate 29.50 149 16271930 81.11 ug/L 98 40) Benzo(a)anthracene 30.76 228 30656697 86.64 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.36 149 22267731 85.36 ug/L 97 42) Chrysene 30.86 228 30504152m 75.03 ug/L 44) Di-n-octylphthalate 33.21 149 31003909m 82.80 ug/L 45) Benzo(b)fluoranthene 33.73 252 28473477 82.56 ug/L 100 46) Benzo(k)fluoranthene 33.82 252 29766745 77.05 ug/L 99 47) Benzo(a)pyrene 34.54 252 26662493 86.42 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.36 276 17959455 87.32 ug/L 99 49) Dibenz(a,h)anthracene 37.48 278 18446576 81.55 ug/L 99 50) Benzo(g,h,i)perylene 38.11 276 18304221 76.22 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL80.D 052202.M Wed May 22 14:46:20 2002 Page 2

NYC-WTC_000013079

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NYC-WTC_000013079Source: NYC Law Department, mirrored locally

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