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Laboratory method parameters and calibration data sheet

Machine-extracted title · confidence 90%

GCMS calibration report for sample AE11602 dated May 30, 2002, showing quantitative results for volatile organic compounds.

NYC-WTC_000013909–000013912

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document yuantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\0 52 8 0 2\CAL5 0.D Vial: 2 Acq On 28 May 2002 12:45 pm Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:45:26 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 30 10:45:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 3 6) Fluoroanthene 26.51 202 26139253 50.33 ug/L 99 3 8) Pyrene 27.14 202 24957044 52.75 ug/L 100 39) Butylbenzylphthalate 29.49 149 10665040 52.67 ug/L 99 40) Benzo(a)anthracene 30.75 228 20038225 56.11 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.35 149 13335659 50.65 ug/L 99 42) Chrysene 30.85 228 20074651m 48.92 ug/L 44) Di-n-octylphthalate 33.20 149 19498336 58.10 ug/L 99 45) Benzo(b)fluoranthene 33.72 252 17522272 56.69 ug/L 100 46) Benzo(k)fluoranthene 33.80 252 19513365 56.36 ug/L 99 4 7) Benzo(a)pyrene 34.52 252 16290473 58.92 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.34 276 10551316m 57.24 ug/L 49) Dibenz(a,h)anthracene 37.46 278 11675357 57.59 ug/L 99 50) Benzo (g,h, i) perylene 38.09 276 11953410 55.53 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL50.D 052202. M Thu May 30,14:15:51 2002 Page 2

NYC-WTC_000013911

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NYC-WTC_000013911Source: NYC Law Department, mirrored locally

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