Laboratory method parameters and calibration data sheet

Quantitation Report (QT Reviewed) Data File . C:\MSDCHEM\1\DATA\052802\CAL5 0.D Vial: 2 Acq On 28 May 2002 12:45 pm Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 14:15 2002 Quant Results File: 052202.RES Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 30 10:45:23 2002 Response via ; Initial Calibration Abundance TIC: CAL50.D

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t £ ii O E O o E Q 500000 CXI co ‘Y t O o CO 0 o Time—> 0- 4.00 6.00 —. r - 8.00 10.00 tM 12.00 --1 14.00 16.00 18.00 1I 20.00 fr Tr 22.00 TIf MTrr 24.00 26.00 28.00 LT r o o o o 30.00 32.00 34.00 36.00 38.00____ o 5 1 Q o CAL50.D 052202.M Thu May 30 14:15:52 2002 Page 3 oo Id > > 7 7