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GC/MS calibration verification results for VOCs, sample AE10895, May 20

Machine-extracted title · confidence 100%

Laboratory report showing calibration data for volatile organic compounds in sample AE10895 analysis.

NYC-WTC_000024058–000024061

Folder label: “GCMS X 5/10/02 A 5/16/02

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NYC 9/11 Public Portal Document yuancitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\0 516 0 2\CAL2 0.D Vial: 2 Acq On 16 May 2002 3:21 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 17 15:13:14 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 13609729 22.19 ug/L 99 3 8) Pyrene 27.17 202 12874448 21.16 ug/L 97 39) Butylbenzylphthalate 29.52 149 5460508 20.14 ug/L # 96 4 0) Benzo(a)anthracene 30.79 228 9416402 19.44 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.38 149 6849064 18.69 ug/L 98 42) Chrysene 30.88 228 9863098 19.66 ug/L 97 44) Di-n-octylphthalate 33.24 149 8995606 18.35 ug/L 98 45) Benzo(b)fluoranthene 33.75 252 9142700 22.74 ug/L 97 46) Benzo(k)fluoranthene 33.83 252 11170579 22.11 ug/L 99 47) Benzo(a)pyrene 34.55 252 8377555 20.87 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.39 276 5826889 20.71 ug/L 99 49) Dibenz(a,h)anthracene 37.51 278 6359048 21.25 ug/L 98 50) Benzo(g,h,i)perylene 38.13 276 7176008 22.84 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL20.D 050102.M Fri May 17 15:13:45 2002 Page 2

NYC-WTC_000024060

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NYC-WTC_000024060Source: NYC Law Department, mirrored locally

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