GCMS analysis results for sample AE11309, May 28, 2002

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Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024997–000025011

Folder label: “GCMS X 5/14/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11308.D Vial: 22 Acq On : 21 May 2002 9:28 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 6 Tetradecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 23.83 0.54 ug/1 37701 Phenanthrene-dl0 25.52 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetradecane 198 C14H30 000629-59-4 90 ' 2 Eicosane 282 C20H42 000112-95-8 90 3 Heptadecane 240 C17H36 000629-78-7 90j 4 Hexadecane 226 C16H34 000544-76-390 Abundance Scan 2051 (23.833 min): 11308.D (-) m/z 57.10 100.00% 43 57 ft 71 __ 5000 85

23,40 23.60 23.80 24.00 24.20 ...... 11 , I . Il 1 । । .< । i i99। ! T i113i ] n i i । i n i p i t i । i i i । । । । । i ] । । i । । । । । i p । । i । । r , , i ................ ............................................. ......................................................................................................................... ................ rn/z 43.05 81.85% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69661: Tetradecane 57 43 71 5000 I 1 1 1 1 I ' ' r1 I 1 ‘ 1 1 I 1 ' 1 1 I 1 1 85 23.40 23.60 23.80 24.00 24.20 m/z 71.10 58.08%

m/z— > I27 . i ' 1 ■ ■ । ■ 1 20 40 +60 80 99 113 II 155 198 T)B—ITi ' 1 ' ' i 1 ' ' ■ i ' 1 ' ' i ' ' ■ ' i ' 1 ' ' i ' ' ' 1 i ' ‘ ' i ' ' ' ' i ' ' 100 120 140 160 180 200 220 240 260 280 Abundance #72324: Eicosane 43 57 90mm 71 23.40 23.60 23.80 24.00 24.20 5000 m/z 41.15 43.54%l 85

99 ... manelasly) I FT 113 141 155169 183197 254 282 m/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280

43 57 #71191: Heptadecane wwe 23.40 23.60 23.80 24.00 24.20 m/z 85.15 34.00% 71 5000 85

m/z-> 1It 20 — 40 I Tun 60 80 100 113127141 I ' ' ' ' I ' 1 ' ' I ' 1 ' ' I ' ' ' ' I ' 1 ' 1 I ' ' 1 1 1 1 1 1 1 I 1 1 1 1 1 1 ' 120 140 160 180 200 220 240 260 280 240 LAA TBl 1 7 I 23.40 23.60 23.80 24.00 24.20 A

11308.D GCMS0520.M Wed May 22 09:21:21 2002 Page 6

NYC-WTC_000025009

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