GCMS analysis results for sample AE11307, May 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\MAY2 10211306.D Vial: 20 Acq On : 21 May 2002 7:30 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 3-Pyrrolidinol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 9.92 0.63 ug/1 40273 1,4-Dichlorobenzene-d4 12.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 9 3 2-Hexanone, 5-methyl- 114 C7H140 000110-12-3 9 4 Acetic/ acid, 1-methylpropyl ester 116 C6H1202 000105-46-4 9 Abundance Scan 532 (9.917 min): 11306. D (-) m/z 43.05 100.00% 43

5000

58 87 1 ' ' i ' ' 98 9.60 9.80 10.00 10.20 1, - nr 14V 51 69 ■' i ' 1 ■ ’ i ''' ■ | ' i 1 .1— m/ z 58.10 20.68% m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #752:3-Pyrrolidinol 43

5000 9.60 9.80 10.00 10.20 57 68 87 m/z 87.05 16.41%| - 1.0 miz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64276:2-Pentanone, 4-hydroxy-4-methyl- 43 9.60 9.80 10,00 10.20 5000 m/ z 41.05 10.77% 58

12738/ . ........ , | ' I ' ' ' 1 I 1 1 1 1 I ' 1 83 101 1 1 ' ' ■ i ' ■ ' 1 i 1 ' ■ ■ 1 1 1 1 1 i'1 1 1 1 I 1 1 ' 1 1 1 m/z-> Abundance 20 30 40

43 50 60 70 80 90 #64147: 2-Hexanone, 5-methyl- 100 110 120 AAAAA MAA 9.60 9.80 ' 1 I 1 1 ‘ ' I ' ' ' 1 I 10.00 10.20 m/z 59.10 10.62%| 58 5000

71 1 - || 8,1 99 114 । i । 1 i p । । । pi i i । ] i i t i ]—i । ! i [ r I—i—i—।—r 1 ■ । 1 1 ' 1 i 1 1 1 1 i 1 ' 1 1 i 1 1 1 1 i m/z—> 20 30 40 50 60 70 80 90 100 110 120 9.60 9.80 10.00 10.20

11306.D GCMS0520.M Wed May 22 09:20:39 2002 Page 2

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