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GCMS analysis results for sample AE10242, May 2002

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Laboratory report documenting GCMS analysis of sample AE10242 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024804–000024812

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document yuantltatlon Report (Q1 Reviewed) Data File : C:\MSDCHEM\l\DATA\020509\10242.D Vial: 20 Acq On : 10 May 2002 5:24 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: Iscint.e Quant Time: May 10 08:27:57 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) | Title : Method 508 GC/MS Scan \ 0 A Last Update : Thu May 09 09:21:01 2002 1 ) ) Response via : Initial Calibration A V 0 DataAcq Meth : 508SCAN1 V (

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 497052 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1890970 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 1010790 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1728301 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1401907 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 880745 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.53 207 51677 6.40 ug/1 -0.04 Spiked Amount 10.000 Recovery = 64.00% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 3605 0.12 ug/1 # 76

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10242.D SCAN020507.M Tue May 14 14:14:46 2002 Page 1

NYC-WTC_000024804

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NYC-WTC_000024804Source: NYC Law Department, mirrored locally

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GCMS sample preparation log, May 2002 · Box DEP Box 18

NYC-WTC_000024427

Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993

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