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GCMS analysis results for sample AE08962, May 7, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08962 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049596–000049608

Folder label: “GCMS X 4/16/02 A 4/24/02

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NYC 9/11 Public Portal Document yuantitatlon Report (QT Reviewed.) Data File : C:\MSDCHEM\1\DATA\020424\08962.D Vial: 13 Acq On : 24 Apr'2002 9:39 pm Operator: Nefliu ' Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: events.e Quant Time: Apr 26 09:54:37 2002 Quant Results File: SCAN020424.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Wed Apr 24 08:54:34 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 8707831 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 33849418 40.00 ug/1 -0.03 17) Acenaphthene-dl0 24.46 164 18728214 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 27533398 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 20212195 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 13316114 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.54 207 886065 8.41 ug/1 -0.03 Spiked Amount 10.000 Recovery = 84.10% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.53 149 73477 0.20 ug/1 # 69

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08962.D SCAN020424.M Fri Apr 26 09:56:33 2002 Page 1

NYC-WTC_000049598

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NYC-WTC_000049598Source: NYC Law Department, mirrored locally

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