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GCMS analysis results for sample AE11278, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024692–000024705

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.152 516 523 563 rBV 844647 1677802 39.70% 6.421% 2 11.370 1400 1411 1430 rBV 1187445 3000543 71.01% 11.484% 3 15.465 2094 2108 2118 rBV2 20902 63832 1.51% 0.244% 4 16.534 2274 2290 2315 rBV 1435317 3769369 89.20% 14.427% 5 22.298 3261 3271 3282 rVB7 8511 21508 0.51% 0.082%

6 24.461 3620 3639 3658 rBV 1417462 3933626 93.09% 15.055% 7 27.551 4143 4165 4178 rBV2 928844 2707159 64.06% 10.361% 8 28.908 4387 4396 4407 rBV7 7991 23463 0.56% 0.090% 9 31.082 4754 4766 4781 rVB5 10630 35951 0.85% 0.138% 10 31.717 4856 4874 4900 rBV2 1366120 4225726 100.00% 16.173%

11 31.952 4908 4914 4922 rVB3 12706 32699 0.77% 0.125% 12 39.931 6262 6272 6296 rBV2 1911294 3723637 88.12% 14.252% 13 40.518 6363 6372 6391 rBV 72039 187127 4.43% 0.716% 14 42.534 6708 6715 6733 rBV5 43245 126164 2.99% 0.483% 15 43.151 6809 6820 6842 rBV2 1259845 2599365 61.51% 9.949%

Sum of corrected areas: 26127971

11278.D SCAN020507.M Thu May 16 09:56:13 2002 Page 1

NYC-WTC_000024696

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NYC-WTC_000024696Source: NYC Law Department, mirrored locally

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