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GCMS sample AE11154 analysis with surrogate recovery, May 2002

Machine-extracted title · confidence 90%

GCMS analysis page for sample AE11154 showing unknown compounds and surrogate compound recovery data.

NYC-WTC_000025556–000025567

Folder label: “GCMS X 5/17/02 A 5/16/02

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Scanned page image, NYC-WTC_000025558
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020515\11154.D Vial: 20 Acq On : 16 May 2002 6:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.117 508 517 519 rBV 30811 45029 1.08% 0.176% 2 6.152 519 523 548 rVB 757270 1393759 33.58% 5.454% 3 11.370 1400 1411 1431 rBV 1185778 2971058 71.59% 11.627% 4 16.534 2274 2290 2308 rBV 1456304 3718817 89.60% 14.553% 5 24.461 3622 3639 3655 rBV2 1397664 3851166 92.79% 15.071%

6 27.551 4146 4165 4180 rBV3 845371 2373197 57.18% 9.287% 7 28.902 4387 4395 4407 rVB8 6735 20783 0.50% 0.081% 8 31.094 4755 4768 4779 rVB4 11194 34884 0.84% 0.137% 9 31.717 4857 4874 4900 rBV2 1401935 4150356 100.00% 16.242% 10 31.946 4906 4913 4925 rBV4 11780 33335 0.80% 0.130%

11 36.441 5667 5678 5692 rBV8 14424 60628 1.46% 0.237% 12 38.715 6056 6065 6080 rBV2 27612 71889 1.73% 0.281% 13 39.931 6258 6272 6295 rBV2 1864817 3652731 88.01% 14.295% 14 40.518 6363 6372 6401 rVB 273560 637845 15.37% 2.496% 15 43.151 6809 6820 6844 rBV 1241864 2537580 61.14% 9.931%

Sum of corrected areas: 25553057

11154 .D SCAN020507.M Thu May 16 14:37:43 2002 Page 1

NYC-WTC_000025558

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NYC-WTC_000025558Source: NYC Law Department, mirrored locally

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