GCMS scan comments for sample AE11480, May 29, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020521\11480 .D Vial: 14 Acq On : 21 May 2002 9:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.349 43 46 52 rBV 18733 24823 0.62% 0.106% 2 3.655 94 98 107 rVB2 23096 35516 0.89% 0.151% 3 6.128 512 519 521 rBV 38121 55598 1.39% 0.237% 4 6.158 521 524 565 rVB 477337 965746 24.17% 4.110% 5 11.375 1401 1412 1433 rBV 1147008 2885266 72.22% 12.280%

6 16.534 2275 2290 2311 rBV 1333982 3592045 89.91% 15.288% 7 24.460 3620 3639 3664 rBV 1315738 3760621 94.13% 16.005% 8 27.551 4145 4165 4178 rBV2 821593 2413711 60.41% 10.273% 9 28.902 4388 4395 4406 rVB6 6657 20576 0.52% 0.088% 10 31.099 4759 4769 4774 rBV5 9790 24827 0.62% 0.106% 11 31.716 4855 4874 4890 rBV2 1326408 3995315 100.00% 17.004% 12 31.957 4907 4915 4929 rVB4 12467 36159 0.91% 0.154% 13 34.813 5394 5401 5412 rVB2 10783 22811 0.57% 0.097% 14 39.930 6261 6272 6292 rBV2 1726026 3437615 86.04% 14.631% 15 43.150 6806 6820 6850 rBV 1072365 2225581 55.70% 9.472%

Sum of corrected areas: 23496210

11480.D SCAN020521.M Fri May 24 09:32:15 2002 Page 1

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