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GCMS analysis results for sample AE11280, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024730–000024742

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020515\11280.D Vial: 14 Acq On : 16 May 2002 12:39 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.158 515 524 558 rBV 906264 1841386 40.92% 6.686% 2 11.375 1401 1412 1430 rBV 1262453 3201094 71.14% 11.622% 3 15.459 2096 2107 2116 rVB3 21422 59748 1.33% 0.217% 4 16.534 2276 2290 2308 rBV 1597678 4015228 89.23% 14.578% 5 24.460 3623 3639 3652 rBV 1526163 4171881 92.71% 15.147%

6 27.551 4146 4165 4180 rBV2 996261 2811421 62.48% 10.207% 7 28.902 4385 4395 4403 rBV6 9141 26637 0.59% 0.097% 8 31.088 4754 4767 4779 rBV3 12008 35633 0.79% 0.129% 9 31.717 4854 4874 4900 TBV2 1497048 4500012 100.00% 16.338% 10 31.946 4906 4913 4923 rVB3 13892 35523 0.79% 0.129%

11 38.532 6027 6034 6042 rBV5 25072 54713 1.22% 0.199% 12 39.931 6260 6272 6294 rBV2 2017878 3793175 84.29% 13.772% 13 40.518 6365 6372 6385 rBV3 77017 192124 4.27% 0.698% 14 43.151 6808 6820 6848 rBV2 1387571 2804396 62.32% 10.182%

Sum of corrected areas: 27542971

11280.D SCAN020507.M Thu May 16 09:59:20 2002 Page 1

NYC-WTC_000024734

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NYC-WTC_000024734Source: NYC Law Department, mirrored locally

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