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GCMS analysis results for sample AE11281, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024706–000024718

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020515\11281.D Vial: 15 Acq On : 16 May 2002 1:38 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.158 516 524 568 rBV 889027 1875433 43.50% 6.831% 2 11.370 1400 1411 1438 rBV 1215443 3126695 72.53% 11.389% 3 15.459 2099 2107 2117 rVB3 17672 46908 1.09% 0.171% 4 16.534 2274 2290 2309 rBV 1507719 3865632 89.67% 14.080% 5 24.461 3617 3639 3654 rBV 1467729 4033045 93.55% 14.690%

6 27.551 4144 4165 4179 rBV2 920305 2701134 62.66% 9.839% 7 28.908 4386 4396 4407 rBV9 7338 23254 0.54% 0.085% 8 31.088 4752 4767 4781 rBV4 9998 36857 0.85% 0.134% 9 31.717 4856 4874 4895 rBV2 1451358 4310920 100.00% 15.702% 10 31.952 4904 4914 4927 rVB5 13170 42393 0.98% 0.154%

11 39.931 6258 6272 6295 rBV2 1918955 3701127 85.85% 13.481% 12 40.518 6364 6372 6389 rBV2 60347 164793 3.82% 0.600% 13 42.540 6702 6716 6748 rBV2 287493 976879 22.66% 3.558% 14 43.151 6807 6820 6841 rBV2 1233225 2549509 59.14% 9.286%

Sum of corrected areas: 27454579

11281.D SCAN020507.M Thu May 16 10:00:52 2002 Page 1

NYC-WTC_000024710

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NYC-WTC_000024710Source: NYC Law Department, mirrored locally

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