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GCMS analysis results for sample AE11304, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11304 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024596–000024612

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024600
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.214 17 23 24 rBV6 10455 17640 0.56% 0.090% 2 3.649 94 97 106 rVB4 10817 16729 0.53% 0.085% 3 5.042 295 334 339 rBV3 30052 232612 7.39% 1.187% 4 6.158 512 524 566 rBV 672829 1332893 42.36% 6.803% 5 7.556 748 762 776 rBV5 9119 42746 1.36% 0.218%

6 11.375 1397 1412 1439 rBV 907230 2284596 72.61% 11.661% 7 11.945 1499 1509 1521 rBV8 6370 18718 0.59% 0.096% 8 16.534 2274 2290 2310 rBV 1080053 2827180 89.85% 14.430% 9 24.455 3622 3638 3651 rBV 1058934 2954660 93.90% 15.081% 10 27.551 4144 4165 4176 rBV3 686759 1986339 63.13% 10.138%

11 31.088 4758 4767 4781 rVB3 7219 19287 0.61% 0.098% 12 31.717 4855 4874 4900 rBV3 1045983 3146581 100.00% 16.060% 13 31.952 4906 4914 4924 rVB5 10046 25995 0.83% 0.133% 14 34.907 5408 5417 5429 rBV6 7529 22126 0.70% 0.113% 15 35.883 5576 5583 5594 rBV2 13597 28033 0.89% 0.143%

16 39.931 6260 6272 6303 rBV2 1383875 2685509 85.35% 13.707% 17 40.518 6364 6372 6394 rBV 66605 174092 5.53% 0.889% 18 43.151 6806 6820 6843 rBV2 863659 1776509 56.46% 9.067%

Sum of corrected areas: 19592245

11304.D SCAN020507.M Fri May 17 13:11:15 2002 Page 1

NYC-WTC_000024600

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NYC-WTC_000024600Source: NYC Law Department, mirrored locally

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