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GCMS analysis results for sample AE11304, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11304 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024596–000024612

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024607
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Llorary searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 6 D-Limonene Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 11.95 0.33 ug/1 18718 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

. 1 D-Limonene 136 C10H16 005989-27-5 64 2 D-Limonene 136 C10H16 005989-27-5 64 3 Limonene 136 C10H16 000138-86-3 59 4 Limonene 136 C10H16 000138-86-3 59 Abundance Scan 1509 (11.945 min): 11304.D (-1499) (-) m/z 67.10 100.00% 67 93

41 79 5000 107 136 ........ | 55 121 ' ‘ I 1 11 1 I 1 1 ■ i ■ ' ■ ■ i ' ' 11.60 11.80 12.00 12.20 - I 86 . m/z 68.10 91.23% ■ ■ i ' ■ • 1 i ■ ' ‘ ■ r 1 I 11 1 1 1' 1 1 1 I1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #21974: D-Limonene 68

93 5000 ......................................... 11.60 11.80 12.00 12.20 41 53 79 121 136 m/ z 93.00 81.18% 107

n/z-> 10 15 20 4 4 ,160., Ipa1... fl I..... Ji , , , 27

30 40 50 60 70 80 90 100 1 1 I 11 11 |1 1 110 TTT—r ■ i > ■ TIIr 120 130 140

.... n..... Abundance #114019: D-Limonene 68 11.60 11.80 12.00 12.20 93 m/z 41.20 50.21% 5000

41 53 79 136 27 107 121 11111111111 i'i । / +161,+ 1 101,85l*... J.... 1.128., IIII n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #114007: Limonene 68 11.60 11.80 12.00 12.20 m/ z 79.00 48.84% 5000 93

41 53 79 27 | .... I . , 11 , . il ' ' I ' ' ' ' I-1-1 1 1 I ' ‘ i1 1 1 , 107 121 136

/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 11.60 11.80 12.00 12.20

11304.D SCAN020507.M Fri May 17 13:11:22 2002 Page 8

NYC-WTC_000024607

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NYC-WTC_000024607Source: NYC Law Department, mirrored locally

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