GCMS analysis results for sample AE11304, May 2002

NYC 9/11 Public Portal Document uiDrrY bearcn compound Report Data File : C:\MSDCHEM\l\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Hexanoic acid Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.56 0.75 ug/1 42746 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanoic acid 116 C6H1202 000142-62-1 64 2 Propanedioic acid, propyl- 146 C6H10O4 000616-62-6 59 3 Pentanoic acid 102 C5H10O2 000109-52-4 59 4 Hexanoic acid 116 C6H1202 000142-62-1 56 Abundance Scan 762 (7.556 min): 11304.D (-748) (-) m/ z 60.10 100.00%

A_ 6b

73 5000 43 55 87 104 A—+—A—4A 7.20 —WAeAn 7.40 7.60 7.80 8.00 " " ।" i •" ■ i ■' ’I’’ ’) -H ’10111111111111117 m/ z 73.00 56.09% m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #113410: Hexanoic acid 60

5000 27 41 73 A... 4 MV4AM4, I u 720 7.40 7.60 7.80 8.00 55 m/z 43.10 36.41% 87 50 1 65 „ । 80 44+ | 92 99

Wokelyihpo, 1 , 36 1" i ‘1 TTH I IIII II TnTHTTTTTT /z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #20103: Propanedioic acid, propyl- 44 63

720 7.40 7.60 7.80 8.00 5000 73 m/z 41.10 23.39% 29 55 39 ""i' -HH +59+4 ,' I' ■' ■i "' ■ I 8■17''i■■'' im 1111711111' 1111 /z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #113416: Pentanoic acid 60 7.20 7.40 7.60 7.80 8.00 m/z 55.00 21.80%

5000 73 41 . 55 .1.47 ||. ! 67 87 103 muupmaun —tmmammppe n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.20 7.40 7.60 7.80 8.00

11304.D SCAN020507.M Fri May 17 13:11:22 2002 Page 7

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