GCMS reference standard results for sample AE10207, May 2002

NYC 9/11 Public Portal Document

‘Data File C:\MSDCHEM\1\DATA\020509\0501REF2.D Vial: 6 Acq On 9 May 2002 3:35 pm Operator: Nefliu Sample 05/01 ref kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 14 14:10:20 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 486219 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1859923 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 985006 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1688786 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1367914 40.00 ug/1 -0.04 44) Perylene-dl2 43.16 264 873912 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.55 207 61618 7.83 ug/1 -0.03 Spiked Amount 10.000 Recovery = 78.30%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.96 74 55629m 7.18 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 306726 16.31 ug/1 98 4) 1.3-Dichlorbenzene 11.11 146 233471 14.87 ug/1 98 5) 1,4-Dichlorobenzene 11.43 146 246517 14.39 ug/1 96 6) 1,2-Dichlorobenzene 11.95 146 237216 15.94 ug/1 97 7) 2,2'oxybis(1-Chloropropane 12.77 45 512779m 17.06 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 234979 17.47 ug/1 98 9) Hexachloroethane 13.25 119 86755 11.67 ug/1 95 11) Nitrobenzene 13.67 77 362575 16.24 ug/1 99 12) Isophorone 14.78 82 746654 19.20 ug/1 98 13) bis(2-Chloroethoxy) methan 16.02 93 390130 16.88 ug/1 95 14) 1,2,4-Trichlorobenzene 16.38 180 208544 15.63 ug/1 98 15) Naphthalene 16.62 128 810177 17.38 ug/1 99 16) Hexachlorobutadiene 17.40 225 100033 12.92 ug/1 92 18) 2-Chloronaphthalene 21.93 162 444537 18.96 ug/1 100 19) Acenaphthylene 23.75 152 745148 16.28 ug/1 99 20) Dimethyl phthalate 23.85 163 547696 17.90 ug/1 98 21) 2,6-Dinitrotoluene 23.96 77 47354 17.98 ug/1 # 91 2 2) Acenaphthene 24.60 153 468066 17.65 ug/1 97 23) 2,4-Dinitrotoluene 25.74 165 109910 15.60 ug/1 92 24) Fluorene 27.01 166 563266 18.46 ug/1 98 25) Diethyl phthalate 27.22 149 612300 19.90 ug/1 99 26) 4-Chlorophenyl-phenylether 27.35 204 263638 17.44 ug/1 96 28) N-Nitrosodiphenylamine 27.94 168 196230 19.74 ug/1 97 29) Azobenzene 28.03 77 762988 16.23 ug/1 99 31) Hexachlorobenzene 29.60 284 162321 18.22 ug/1 100 32) 4-Bromophenyl-phenylether 29.71 248 156176 17.91 ug/1 87 33) Phenanthrene 31.82 178 782212 18.21 ug/1 98 34) Anthracene 32.05 178 727800 16.73 ug/1 98 35) Di-n-butylphthalate 34.81 149 995340 18.52 ug/1 99

(#) = qualifier out of range (m) = manual integration 0501REF2.D SCAN020507.M Tue May 14 14:10:54 2002 Page 1

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